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kp-sil [40+m] column cartridges  (BIOTAGE)

 
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    Structured Review

    BIOTAGE kp-sil [40+m] column cartridges
    Kp Sil [40+M] Column Cartridges, supplied by BIOTAGE, used in various techniques. Bioz Stars score: 90/100, based on 1 PubMed citations. ZERO BIAS - scores, article reviews, protocol conditions and more
    https://www.bioz.com/product/40+m+cartridge/flash+12+++flash+25++or+flash+40++columns+charged+with+kp+sil++40+63+%C2%B5m++pore+diameter+60+%C3%A5+/pm31685332-216-18-14
    Average 90 stars, based on 1 article reviews
    kp-sil [40+m] column cartridges - by Bioz Stars, 2026-09
    90/100 stars

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    Related Articles

    other:

    Article Title: (3,4-disubstituted)propanoic carboxylates as S1P (Edg) receptor agonists
    Article Snippet: Chromatography on a Biotage 40 M cartridge using 3:1 hexanes/acetone as the eluant afforded 1.84 g of the title compound: ESI-MS (m/z) 242.1, 244.1; HPLC A: 2.22 min.

    Article Title: 7-phenoxychroman carboxylic acid derivatives
    Article Snippet: The reaction was cooled and loaded directly onto a biotage 40 M cartridge, eluting with 20% ethyl acetate/hexanes to 100% ethyl acetate to yield 1 g of the crude product which was found to contain NMP.

    Article Title: HPTS-mono and bis Cys-MA polymerizable fluorescent dyes for use in analyte sensors
    Article Snippet: The residue was mixed with silica gel (3 g) and crushed into a fine powder and dry loaded onto a Biotage 40 M cartridge.

    Article Title: Edg receptor agonists
    Article Snippet: Chromatography on a Biotage 40 M cartridge using hexanes (1L), then 4:1 v/v hexanes/CH2Cl2 (1 L) as the eluant afforded 5.10 g (78%) of the title compound: 1H NMR (400 Mhz) δ 1.40 (t, J=7.2, 3H), 4.39 (q, J=7.2, 2H), 7.42 (app s, 5H), 7.74 (q, J=1.6, 1H).

    Article Title: (3,4-disubstituted)propanoic carboxylates as S1P (Edg) receptor agonists
    Article Snippet: Chromatography on a Biotage 40 M cartridge using 9:1 v/v hexanes/EtOAc, the 7:3 v/v hexanes/EtOAc as the eluant afforded 2.55 g of impure product.

    Article Title: (3,4-disubstituted)propanoic carboxylates as S1P (Edg) receptor agonists
    Article Snippet: Chromatography on a Biotage 40 M cartridge using hexanes as the eluant afforded 1.11 g of the title compound: 1H NMR (500 MHz, CDCl3) δ 8.14 (d, J=2.0, 1H), 8.64 (d, J=2.0, 1H).

    Chromatography:

    Article Title: 2-(aryl)azacyclylmethyl carboxylates, sulfonates, phosphonates, phosphinates and heterocycles as S1P receptor agonists
    Article Snippet: .. Chromatography on a Biotage 40+M cartridge using 9:1 v/v EtOAc/CH3OH as the eluant gave 2.68 g (100%) of the title compound containing trace amount of DMF: 1H NMR (CD3OD) δ 1.90-1.97 (m, 1H), 2.43-2.51 (m, 2H), 2.60-2.67 (m, 1H), 4.85 (t, J=7.2, 1H), 7.41 (d, J=8.8, 2H), 7.65 (d, J=8.5, 2H). ..

    Article Title: 2-(aryl)azacyclylmethyl carboxylates, sulfonates, phosphonates, phosphinates and heterocycles as S1P receptor agonists
    Article Snippet: .. Chromatography on a Biotage 40+M cartridge using 1:19 v/v EtOAc/hexanes as the eluant afforded 1.77 g (100%) of the title compound: 1H NMR δ 1.41 (d, J=6.2, 6H), 4.63-4.70 (m, 1H), 6.93 (d, J=8.7, 1H), 7.89 (dd, J=2.2, 8.6, 1H), 8.05 (d, J=2.0, 1H). ..

    Nuclear Magnetic Resonance:

    Article Title: 2-(aryl)azacyclylmethyl carboxylates, sulfonates, phosphonates, phosphinates and heterocycles as S1P receptor agonists
    Article Snippet: .. Chromatography on a Biotage 40+M cartridge using 9:1 v/v EtOAc/CH3OH as the eluant gave 2.68 g (100%) of the title compound containing trace amount of DMF: 1H NMR (CD3OD) δ 1.90-1.97 (m, 1H), 2.43-2.51 (m, 2H), 2.60-2.67 (m, 1H), 4.85 (t, J=7.2, 1H), 7.41 (d, J=8.8, 2H), 7.65 (d, J=8.5, 2H). ..

    Article Title: 2-(aryl)azacyclylmethyl carboxylates, sulfonates, phosphonates, phosphinates and heterocycles as S1P receptor agonists
    Article Snippet: .. Chromatography on a Biotage 40+M cartridge using 1:19 v/v EtOAc/hexanes as the eluant afforded 1.77 g (100%) of the title compound: 1H NMR δ 1.41 (d, J=6.2, 6H), 4.63-4.70 (m, 1H), 6.93 (d, J=8.7, 1H), 7.89 (dd, J=2.2, 8.6, 1H), 8.05 (d, J=2.0, 1H). ..



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